Chemistry 7750
Electroanalytical Chemistry

Fall 2009

Course Meeting Time

TTh 1:30-3:00 pm

212 Choppin Hall

And as needed

 

 

 

 



 

Syllabus for Fall 2009

 

Lecture Number

Tentative Date

Topic

Complete Notes are Posted Here

Pages of Notes Covered

Reading Assignment in Bard and Faulkner

(Ahead of Time)

 

Homework Assignment in B&F

HW Due Lecture

Quiz

0

8-25 Course Overview
and
Preparation for First Lecture
 
  1.1 to 1.1.2, 1.3, 1.4 to 1.4.2, 4.1, 4.2, 4.3 to 4.3.1, 4.3.2, 4.4 to 4.4.3 None   #0

1

8-27 Basics of Electrochemistry   2.1, 2.2 4.3, 4.5
 
3 #1

2

9-1 Basics of Electrochemistry   2.3, 1.1.2, 1.1.2, 1.2,  1.4.2, 1.4.3     #2
3 9-3 Basics of Electrochemistry   Read/Re-read 1.3 and 1.4 2.1 (except g), 2.3, 2.4
 
5 #3

4

9-8 Basics of Electrochemistry   3.1 to 3.4.5 1.1,1.2,1.5,1.6,1.7 7 #4

5

9-15 Kinetics of Electron Transfer - Also skim over AC A-page Article   3.4.5, 3.5 to 3.5.2
 

 
  #5

6

9-17 Kinetics of Electron Transfer   Carefully read the Analytical Chemistry
A-page article, including pertinent references
    #6

7

9-22 Discussion of
AC A-page Article
  Prepare for Exam I     #7

E-1

9-24

Examination I
Covering
  Lectures 0-7
Key

  13.1 to 13.3.3

 

 

     

8

9-29

The Electrochemical Double Layer

 

  13.3.3  to 13.4   13.6,  13.7, 13.12 10 #8 

9

10-6

The Electrochemical Double Layer

and discussion of

Nanoelectrode paper

 

  5.1 to 5.2.2     #9

10

10-8 Potential Step Methods   5.4 to 5.4.2,
5.5 to 5.5.2
No assigned HW   #10

11

10-13 Potential Step Methods

 

  5.7 to 5.8.3     #11

12

10-15 Potential Step Methods

DPSCA paper on Cobalamins

DPSCC BAS Tutorial

 

  All of Chapter 7 (B&F);
Chapters 5 and 19 in Heineman and Kissinger
    #12

13

10-21  Polarographic and Pulsed Voltammetric Methods

Handout on Stripping Analysis

Paper on OSWV-Stripping

        #13
14 10-22 Discussion of Articles on Pulsed Methods and Stripping Analysis   Prepare for Exam II     No Quiz
E-2 10-27

Examination II
  Covering Lectures
 8-14
Key
  

  6.1-6.2.2, 6.2.4-6.3.2      

15

10-29 Potential Sweep Methods-LSV
 
  6.2.3,
6.5-6.6,
12.3.3 to 12.3.3b
Supplementary Materials for Cyclic Voltammetry
6.4, 6.5, 6.6, 6.9, 6.12a 17 #15

16

11-03 Potential Sweep Methods-CV   9.1 to 9.4
9.4 to 9.5
review 9.2.2
9.8 to 9.8.2

 

13.5 to 13.5.3, 13.7 to End of Chp. 13, 14.3.2

    #16
17 11-05 Hydrodynamic Voltammetry Methods     5.2.2, 5.2.3, all of 5.3  up to 5.4
and
Microelectrode Book Chapter by Pletcher
 
  #17

18

11-10 Electrodes of Submillimeter Dimensions - General Properties     Microelectrode Book Chapter by McCarley
and
Arrigan Review Article
  #18

19

11-12 Electrodes of Submillimeter Dimensions - Fabrication Routes

 

        #19

20

11-17 Electrodes of Submillimeter Dimensions - Fabrication Routes     1.Nanobattery Paper
2.Murray Review
3.E-beam Fabrication Paper
4.NanoDiscElectrode Paper
 
  No Quiz

21

11-19

Modified Electrodes

    Murray Book Chapter   #21 

 E-3

12-01 Examination III
Covering Lectures 15-21
         

22

12-03 Practical Aspects of Electrochemistry at Solid Electrodes
 
         

F-1

12-9

Final Exam
Wednesday, December 9 at
10 am

         

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 


 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 
 
 
 


Copyright 1998-2009
Louisiana State University, Department of Chemistry.
All Rights Reserved.

Last Revised: 11/30/2009 10:33:31 AM